¹³C solvent peaks

Solvent CDCl₃ (CD₃)₂CO (CD₃)₂SO C₆D₆ CD₃CN CD₃OD D₂O

solvent signals 77.16 29.84
206.26 39.52 128.06 1.32
118.26 49.00 -

acetic acid 175.99
20.81 172.31
20.51 171.93
20.95 175.82
20.37 173.21
20.73 175.11
20.56 177.21
21.03

acetone 207.07
30.92 205.87
30.60 206.31
30.56 204.43
30.14 207.43
30.91 209.67
30.67 215.94
30.89

acetonitrile 116.43
1.89 117.60
1.12 117.91
1.03 116.02
0.20 118.26
1.79 118.06
0.85 119.68
1.47

benzene 128.37 129.15 128.30 128.62 129.32 129.34 -

tert-butyl alcohol 69.15
31.25 68.13
30.72 66.88
30.38 68.19
30.47 68.74
30.68 69.40
30.91 70.36
30.29

tert-butyl methyl ether 49.45
72.87
26.99 49.35
72.81
27.24 48.70
72.04
26.79 49.19
72.40
27.09 49.52
73.17
27.28 49.66
74.32
27.22 49.37
75.62
26.60

BHT (2,6-Dimethyl- 4-tert-butylphenol) 151.55
135.87
125.55
128.27
21.20
30.33
34.25 152.51
138.19
129.05
126.03
21.31
31.61
35.00 151.47
139.12
127.97
124.85
20.97
31.25
34.33 152.05
136.08
128.52
125.83
21.40
31.34
34.35 152.42
138.13
129.61
126.38
21.23
31.50
35.05 152.85
139.09
129.49
126.11
21.38
31.15
35.36 -

chloroform 77.36 79.19 79.16 77.79 79.17 79.44 -

cyclohexane 26.94 27.51 26.33 27.23 27.63 27.96 -

1,2-dichloroethane 43.50 45.25 45.02 43.59 45.54 45.11 -

dichloromethane 53.52 54.95 54.84 53.46 55.32 54.78 -

diethyl ether 15.20
65.91 15.78
66.12 15.12
62.05 15.46
65.94 15.63
66.32 15.46
66.88 14.77
66.42

diglyme 59.01
70.51
71.90 58.77
71.03
72.63 57.98
69.54
71.25 58.66
70.87
7.35 58.90
70.99
72.63 59.06
71.33
72.92 58.67
70.05
71.63

1,2-dimethoxyethane 59.08
71.84 58.45
72.47 58.01
17.07 58.68
72.21 58.89
72.47 59.06
72.72 58.67
71.49

dimethylacetamide 21.53
171.07
35.28
38.13 21.51
170.61
34.89
37.92 21.29
169.54
37.38
34.42 21.16
169.95
34.67
37.03 21.76
171.31
35.17
38.26 21.32
173.32
35.50
38.43 21.09
174.57
35.03
38.76

dimethylformamide 162.62
36.50
31.45 162.79
36.15
31.03 162.29
35.73
30.73 162.13
35.25
30.72 163.31
36.57
31.32 164.73
36.89
31.61 165.53
37.54
32.03

dimethylsulfoxide 40.76 41.23 40.45 40.03 41.31 40.45 39.39

dioxane 67.14 67.60 66.36 67.16 67.72 68.11 67.19

ethanol 18.41
58.28 18.89
57.72 18.51
56.07 18.72
57.86 18.80
57.96 18.40
58.26 17.47
58.05

ethyl acetate 21.04
171.36
60.49
14.19 20.83
170.96
60.56
14.50 20.68
170.31
59.74
14.40 20.56
170.44
60.21
14.19 21.16
171.68
60.98
14.54 20.88
172.89
61.50
14.49 21.15
175.26
62.32
13.92

ethyl methyl ketone 29.49
209.56
36.89
7.86 29.30
208.30
36.75
8.03 29.26
208.72
35.83
7.61 28.56
206.55
36.36
7.91 29.60
209.88
37.09
8.14 29.39
212.16
37.34
8.09 29.49
218.43
37.27
7.87

ethylene glycol 63.79 64.26 62.76 64.34 64.22 64.30 63.17

grease 29.76 30.73 29.20 30.21 30.86 31.29 -

n-hexane 14.14
22.70
31.64 14.34
23.38
32.30 13.88
22.05
30.95 14.32
23.04
31.96 14.43
23.40
32.36 14.45
23.68
32.73 -

HMPA 36.87 37.04 36.42 36.88 37.10 37.00 36.46

methanol 50.41 49.77 48.59 49.97 49.90 49.86 49.50

nitromethane 62.50 63.21 63.28 61.16 63.66 63.08 63.22

n-pentane 14.08
22.38
34.16 14.29
22.98
34.83 13.28
21.70
33.48 14.25
22.72
34.45 14.37
23.08
34.89 14.39
23.38
35.30 -

2-propanol 25.14
64.50 25.67
63.85 25.43
64.92 25.18
64.23 25.55
64.30 25.27
64.71 24.38
64.88

pyridine 149.90
123.75
135.96 150.67
124.57
136.56 149.58
123.84
136.05 150.27
123.58
135.28 150.76
127.76
136.89 150.07
125.53
138.35 149.18
125.12
138.27

silicone grease 1.04 1.40 - 1.38 - 2.10 -

tetrahydrofuran 25.62
67.97 26.15
68.07 25.14
67.03 25.72
67.80 26.27
68.33 26.48
68.83 25.67
68.68

toluene 21.46
137.89
129.07
128.26
125.33 21.46
138.48
129.76
129.03
126.12 20.99
137.35
128.88
128.18
125.29 21.10
137.91
129.33
128.56
125.68 21.50
138.90
129.94
129.23
126.28 21.50
138.85
129.91
129.20
126.29 -

triethylamine 11.61
46.25 12.49
47.07 11.74
45.74 12.35
46.77 12.38
47.10 11.09
46.96 9.07
47.19

Solvent CDCl₃ (CD₃)₂CO (CD₃)₂SO C₆D₆ CD₃CN CD₃OD D₂O

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Solvent	CDCl₃	(CD₃)₂CO	(CD₃)₂SO	C₆D₆	CD₃CN	CD₃OD	D₂O
solvent signals	77.16	29.84 206.26	39.52	128.06	1.32 118.26	49.00	-
acetic acid	175.99 20.81	172.31 20.51	171.93 20.95	175.82 20.37	173.21 20.73	175.11 20.56	177.21 21.03
acetone	207.07 30.92	205.87 30.60	206.31 30.56	204.43 30.14	207.43 30.91	209.67 30.67	215.94 30.89
acetonitrile	116.43 1.89	117.60 1.12	117.91 1.03	116.02 0.20	118.26 1.79	118.06 0.85	119.68 1.47
benzene	128.37	129.15	128.30	128.62	129.32	129.34	-
tert-butyl alcohol	69.15 31.25	68.13 30.72	66.88 30.38	68.19 30.47	68.74 30.68	69.40 30.91	70.36 30.29
tert-butyl methyl ether	49.45 72.87 26.99	49.35 72.81 27.24	48.70 72.04 26.79	49.19 72.40 27.09	49.52 73.17 27.28	49.66 74.32 27.22	49.37 75.62 26.60
BHT (2,6-Dimethyl- 4-tert-butylphenol)	151.55 135.87 125.55 128.27 21.20 30.33 34.25	152.51 138.19 129.05 126.03 21.31 31.61 35.00	151.47 139.12 127.97 124.85 20.97 31.25 34.33	152.05 136.08 128.52 125.83 21.40 31.34 34.35	152.42 138.13 129.61 126.38 21.23 31.50 35.05	152.85 139.09 129.49 126.11 21.38 31.15 35.36	-
chloroform	77.36	79.19	79.16	77.79	79.17	79.44	-
cyclohexane	26.94	27.51	26.33	27.23	27.63	27.96	-
1,2-dichloroethane	43.50	45.25	45.02	43.59	45.54	45.11	-
dichloromethane	53.52	54.95	54.84	53.46	55.32	54.78	-
diethyl ether	15.20 65.91	15.78 66.12	15.12 62.05	15.46 65.94	15.63 66.32	15.46 66.88	14.77 66.42
diglyme	59.01 70.51 71.90	58.77 71.03 72.63	57.98 69.54 71.25	58.66 70.87 7.35	58.90 70.99 72.63	59.06 71.33 72.92	58.67 70.05 71.63
1,2-dimethoxyethane	59.08 71.84	58.45 72.47	58.01 17.07	58.68 72.21	58.89 72.47	59.06 72.72	58.67 71.49
dimethylacetamide	21.53 171.07 35.28 38.13	21.51 170.61 34.89 37.92	21.29 169.54 37.38 34.42	21.16 169.95 34.67 37.03	21.76 171.31 35.17 38.26	21.32 173.32 35.50 38.43	21.09 174.57 35.03 38.76
dimethylformamide	162.62 36.50 31.45	162.79 36.15 31.03	162.29 35.73 30.73	162.13 35.25 30.72	163.31 36.57 31.32	164.73 36.89 31.61	165.53 37.54 32.03
dimethylsulfoxide	40.76	41.23	40.45	40.03	41.31	40.45	39.39
dioxane	67.14	67.60	66.36	67.16	67.72	68.11	67.19
ethanol	18.41 58.28	18.89 57.72	18.51 56.07	18.72 57.86	18.80 57.96	18.40 58.26	17.47 58.05
ethyl acetate	21.04 171.36 60.49 14.19	20.83 170.96 60.56 14.50	20.68 170.31 59.74 14.40	20.56 170.44 60.21 14.19	21.16 171.68 60.98 14.54	20.88 172.89 61.50 14.49	21.15 175.26 62.32 13.92
ethyl methyl ketone	29.49 209.56 36.89 7.86	29.30 208.30 36.75 8.03	29.26 208.72 35.83 7.61	28.56 206.55 36.36 7.91	29.60 209.88 37.09 8.14	29.39 212.16 37.34 8.09	29.49 218.43 37.27 7.87
ethylene glycol	63.79	64.26	62.76	64.34	64.22	64.30	63.17
grease	29.76	30.73	29.20	30.21	30.86	31.29	-
n-hexane	14.14 22.70 31.64	14.34 23.38 32.30	13.88 22.05 30.95	14.32 23.04 31.96	14.43 23.40 32.36	14.45 23.68 32.73	-
HMPA	36.87	37.04	36.42	36.88	37.10	37.00	36.46
methanol	50.41	49.77	48.59	49.97	49.90	49.86	49.50
nitromethane	62.50	63.21	63.28	61.16	63.66	63.08	63.22
n-pentane	14.08 22.38 34.16	14.29 22.98 34.83	13.28 21.70 33.48	14.25 22.72 34.45	14.37 23.08 34.89	14.39 23.38 35.30	-
2-propanol	25.14 64.50	25.67 63.85	25.43 64.92	25.18 64.23	25.55 64.30	25.27 64.71	24.38 64.88
pyridine	149.90 123.75 135.96	150.67 124.57 136.56	149.58 123.84 136.05	150.27 123.58 135.28	150.76 127.76 136.89	150.07 125.53 138.35	149.18 125.12 138.27
silicone grease	1.04	1.40	-	1.38	-	2.10	-
tetrahydrofuran	25.62 67.97	26.15 68.07	25.14 67.03	25.72 67.80	26.27 68.33	26.48 68.83	25.67 68.68
toluene	21.46 137.89 129.07 128.26 125.33	21.46 138.48 129.76 129.03 126.12	20.99 137.35 128.88 128.18 125.29	21.10 137.91 129.33 128.56 125.68	21.50 138.90 129.94 129.23 126.28	21.50 138.85 129.91 129.20 126.29	-
triethylamine	11.61 46.25	12.49 47.07	11.74 45.74	12.35 46.77	12.38 47.10	11.09 46.96	9.07 47.19
Solvent	CDCl₃	(CD₃)₂CO	(CD₃)₂SO	C₆D₆	CD₃CN	CD₃OD	D₂O