¹H solvent peaks

-

Solvent Multiplicity CDCl₃ (CD₃)₂CO (CD₃)₂SO C₆D₆ CD₃CN CD₃OD D₂O

solvent residual peak 7.26 2.05 2.50 7.16 1.94 3.31 4.79

H₂O s 1.56 2.84 3.33 0.40 2.13 4.87 -

acetic acid s 2.10 1.96 1.91 1.55 1.96 1.99 2.08

acetone s 2.17 2.09 2.09 1.55 2.08 2.15 2.22

acetonitrile s 2.10 2.05 2.07 1.55 1.96 2.03 2.06

benzene s 7.36 7.36 7.37 7.15 7.37 7.33 -

n-Butanol t, 6
t, 7 3.67
0.94 - 3.41
0.89 - - 3.54
0.93 3.60
0.89

tert-butyl alcohol s
s 1.28 1.18 1.11
4.19 1.05
1.55 1.16
2.18 1.40 1.24

tert-butyl methyl ether s
s 1.19
3.22 1.13
3.13 1.11
3.08 1.07
3.04 1.14
3.13 1.15
3.20 1.21
3.22

2,6-Dimethyl- 4-tert-butylphenol s
s
s
s 6.98
5.01
2.27
1.43 6.96

2.22
1.41 6.87
6.65
2.18
1.36 7.05
4.79
2.24
1.38 6.97
5.20
2.22
1.39 6.92

2.21
1.40 -

Chloroacetic Acid s 4.14 - 4.28 - - - 4.25

chloroform s 7.26 8.02 8.32 6.15 7.58 7.90 -

cyclohexane s 1.43 1.43 1.40 1.40 1.44 1.45 -

1,2-Dibromoethane s 3.63 - 3.84 - - 3.72 3.79

Dichloroacetic Acid s 5.98 6.68 - - - 6.21

1,2-dichloroethane s 3.73 3.87 3.90 2.90 3.81 3.78 -

dichloromethane s 5.30 5.63 5.76 4.27 5.44 5.49 -

Diethyleneglycol,
dimethyl Ether m
s 3.60 (m)
3.38 - 3.49 (m)
3.28 - - 3.63 (m)
3.37

diethyl ether t, 7
q, 7 1.21
3.48 1.11
3.41 1.09
3.38 1.11
3.26 1.12
3.42 1.18
3.49 1.17
3.56

diglyme m
m
s 3.65
3.57
3.39 3.56
3.47
3.28 3.51
3.38
3.24 3.46
3.34
3.11 3.53
3.45
3.29 3.61
3.58
3.35 3.67
3.61
3.37

Diisopropyl Ether d, 6 1.12 (d,6) - 1.04 (d,6) - - - 1.12 (d,6)

1,2-dimethoxyethane s
s 3.40
3.55 3.28
3.46 3.24
3.43 3.12
3.33 3.28
3.45 3.35
3.52 3.37
3.60

dimethylacetamide s
s
s 2.09
3.02
2.94 1.97
3.00
2.83 1.96
2.94
2.78 1.60
2.57
2.05 1.97
2.96
2.83 2.07
3.31
2.92 2.08
3.06
2.90

dimethylformamide s
s
s 8.02
2.96
2.88 7.96
2.94
2.78 7.95
2.89
2.73 7.63
2.36
1.86 7.92
2.89
2.77 7.97
2.99
2.86 7.92
3.01
2.85

dimethylsulfoxide s 2.62 2.52 2.54 1.68 2.50 2.65 2.71

dioxane s 3.71 3.59 3.57 3.35 3.60 3.66 3.75

Ethanediol s 3.76 - 3.42 - - - 3.66

ethanol t, 7
q, 7
s 1.25
3.72
1.32 1.12
3.57
3.39 1.06
3.44
4.63 0.96
3.34 1.12
3.54
2.47 1.19
3.60 1.17
3.65

ethyl acetate s
q, 7
t, 7 2.05
4.12
1.26 1.97
4.05
1.20 1.99
4.03
1.17 1.65
3.89
0.92 1.97
4.06
1.20 2.01
4.09
1.24 2.07
4.14
1.24

ethyl methyl ketone s
q, 7
t, 7 2.14
2.46
1.06 2.07
2.45
0.96 2.07
2.43
0.91 1.58
1.81
0.85 2.06
2.43
0.96 2.12
2.50
1.01 2.19
3.18
1.26

ethylene glycol s 3.76 3.28 3.34 3.41 3.51 3.59 3.65

Ethyl Formate s
q, 7
1.29 (t, 7) 8.04
4.22
1.29 - 8.23
4.17
1.24 - - - 8.16
4.28
1.29

Formic Acid s 8.02 - 8.18 - - - 8.22

grease m
br s 0.86
1.26 0.87
1.29 - 0.92
1.36 0.86
1.27 0.88
1.29 -

n-hexane t
m 0.88
1.26 0.88
1.28 0.86
1.25 0.89
1.24 0.89
1.28 0.90
1.29 -

HMPA d, 9.5 2.65 2.59 2.53 2.40 2.57 2.64 2.61

Isobutyl Methyl Ketone s
d, 6 2.12
0.92 - 2.08
0.88 - - 2.11
0.91 2.19
0.88

Isopropyl Alcohol m
d, 6 4.03
1.20 - -
1.06 - - 3.92
1.14 -
1.18

methanol s
s 3.49
1.09 3.31
3.12 3.16
4.01 3.07 3.28
2.16 3.34 3.34

Methyl Acetate s
s 3.67
2.05 - 3.61
1.92 - - - 3.68
2.09

Methyl Iodide s 2.16 - 2.21 - - 2.15 insol

Morpholine m
m 3.69
2.85 - 3.52
2.68 - 3.64
2.79 3.70
2.79

nitromethane s 4.33 4.43 4.42 2.94 4.31 4.34 4.40

n-pentane t, 7
m 0.88
1.27 0.88
1.27 0.86
1.27 0.87
1.23 0.89
1.29 0.90
1.29 -

Propane-1,2-diol d, 6 1.17 - 1.04 - - - 1.13

Propionoic Acid q, 7
t, 7 2.42
1.18 - 2.26
1.03 - - - 2.47
1.10

2-propanol d, 6
sep, 6 1.22
4.04 1.10
3.90 1.04
3.78 0.95
3.67 1.09
3.87 1.50
3.92 1.17
4.02

pyridine m
m
m 8.62
7.29
7.68 8.58
7.35
7.76 8.58
7.39
7.79 8.53
6.66
6.98 8.57
7.33
7.73 8.53
7.44
7.85 8.52
7.45
7.87

Pyridine.HCl m
m
m - - - - - 8.92
8.19
8.69 -

silicone grease s 0.07 0.13 - 0.29 0.08 0.10 -

Succinimide s 2.75 - 2.63 - - - 2.78

1,1,2,2-Tetrachloroethane s 5.96 - 6.92 - - - insol

tetrahydrofuran m
m 1.85
3.76 1.79
3.63 1.76
3.60 1.40
3.57 1.80
3.64 1.87
3.71 1.88
3.74

toluene s
m
m 2.36
7.17
7.25 2.32
7.1-7.2
7.1-7.2 2.30
7.18
7.25 2.11
7.02
7.13 2.33
7.1-7.3
7.1-7.3 2.32
7.16
7.16 -

1,1,1-Trichloroethane s 2.72 - 2.80 - - - insol

triethylamine t, 7
q, 7 1.03
2.53 0.96
2.45 0.93
2.43 0.96
2.40 0.96
2.45 1.05
2.58 0.99
2.57

Water s 1.60 - 3.40 - - - 4.60

Solvent Multiplicity CDCl₃ (CD₃)₂CO (CD₃)₂SO C₆D₆ CD₃CN CD₃OD D₂O

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Solvent	Multiplicity	CDCl₃	(CD₃)₂CO	(CD₃)₂SO	C₆D₆	CD₃CN	CD₃OD	D₂O
solvent residual peak		7.26	2.05	2.50	7.16	1.94	3.31	4.79
H₂O	s	1.56	2.84	3.33	0.40	2.13	4.87	-
acetic acid	s	2.10	1.96	1.91	1.55	1.96	1.99	2.08
acetone	s	2.17	2.09	2.09	1.55	2.08	2.15	2.22
acetonitrile	s	2.10	2.05	2.07	1.55	1.96	2.03	2.06
benzene	s	7.36	7.36	7.37	7.15	7.37	7.33	-
n-Butanol	t, 6 t, 7	3.67 0.94	-	3.41 0.89	-	-	3.54 0.93	3.60 0.89
tert-butyl alcohol	s s	1.28	1.18	1.11 4.19	1.05 1.55	1.16 2.18	1.40	1.24
tert-butyl methyl ether	s s	1.19 3.22	1.13 3.13	1.11 3.08	1.07 3.04	1.14 3.13	1.15 3.20	1.21 3.22
2,6-Dimethyl- 4-tert-butylphenol	s s s s	6.98 5.01 2.27 1.43	6.96 2.22 1.41	6.87 6.65 2.18 1.36	7.05 4.79 2.24 1.38	6.97 5.20 2.22 1.39	6.92 2.21 1.40	-
Chloroacetic Acid	s	4.14	-	4.28	-	-	-	4.25
chloroform	s	7.26	8.02	8.32	6.15	7.58	7.90	-
cyclohexane	s	1.43	1.43	1.40	1.40	1.44	1.45	-
1,2-Dibromoethane	s	3.63	-	3.84	-	-	3.72	3.79
Dichloroacetic Acid	s	5.98		6.68	-	-	-	6.21
1,2-dichloroethane	s	3.73	3.87	3.90	2.90	3.81	3.78	-
dichloromethane	s	5.30	5.63	5.76	4.27	5.44	5.49	-
Diethyleneglycol, dimethyl Ether	m s	3.60 (m) 3.38	-	3.49 (m) 3.28	-	-		3.63 (m) 3.37
diethyl ether	t, 7 q, 7	1.21 3.48	1.11 3.41	1.09 3.38	1.11 3.26	1.12 3.42	1.18 3.49	1.17 3.56
diglyme	m m s	3.65 3.57 3.39	3.56 3.47 3.28	3.51 3.38 3.24	3.46 3.34 3.11	3.53 3.45 3.29	3.61 3.58 3.35	3.67 3.61 3.37
Diisopropyl Ether	d, 6	1.12 (d,6)	-	1.04 (d,6)	-	-	-	1.12 (d,6)
1,2-dimethoxyethane	s s	3.40 3.55	3.28 3.46	3.24 3.43	3.12 3.33	3.28 3.45	3.35 3.52	3.37 3.60
dimethylacetamide	s s s	2.09 3.02 2.94	1.97 3.00 2.83	1.96 2.94 2.78	1.60 2.57 2.05	1.97 2.96 2.83	2.07 3.31 2.92	2.08 3.06 2.90
dimethylformamide	s s s	8.02 2.96 2.88	7.96 2.94 2.78	7.95 2.89 2.73	7.63 2.36 1.86	7.92 2.89 2.77	7.97 2.99 2.86	7.92 3.01 2.85
dimethylsulfoxide	s	2.62	2.52	2.54	1.68	2.50	2.65	2.71
dioxane	s	3.71	3.59	3.57	3.35	3.60	3.66	3.75
Ethanediol	s	3.76	-	3.42	-	-	-	3.66
ethanol	t, 7 q, 7 s	1.25 3.72 1.32	1.12 3.57 3.39	1.06 3.44 4.63	0.96 3.34	1.12 3.54 2.47	1.19 3.60	1.17 3.65
ethyl acetate	s q, 7 t, 7	2.05 4.12 1.26	1.97 4.05 1.20	1.99 4.03 1.17	1.65 3.89 0.92	1.97 4.06 1.20	2.01 4.09 1.24	2.07 4.14 1.24
ethyl methyl ketone	s q, 7 t, 7	2.14 2.46 1.06	2.07 2.45 0.96	2.07 2.43 0.91	1.58 1.81 0.85	2.06 2.43 0.96	2.12 2.50 1.01	2.19 3.18 1.26
ethylene glycol	s	3.76	3.28	3.34	3.41	3.51	3.59	3.65
Ethyl Formate	s q, 7 1.29 (t, 7)	8.04 4.22 1.29	-	8.23 4.17 1.24	-	-	-	8.16 4.28 1.29
Formic Acid	s	8.02	-	8.18	-	-	-	8.22
grease	m br s	0.86 1.26	0.87 1.29	-	0.92 1.36	0.86 1.27	0.88 1.29	-
n-hexane	t m	0.88 1.26	0.88 1.28	0.86 1.25	0.89 1.24	0.89 1.28	0.90 1.29	-
HMPA	d, 9.5	2.65	2.59	2.53	2.40	2.57	2.64	2.61
Isobutyl Methyl Ketone	s d, 6	2.12 0.92	-	2.08 0.88	-	-	2.11 0.91	2.19 0.88
Isopropyl Alcohol	m d, 6	4.03 1.20	-	- 1.06	-	-	3.92 1.14	- 1.18
methanol	s s	3.49 1.09	3.31 3.12	3.16 4.01	3.07	3.28 2.16	3.34	3.34
Methyl Acetate	s s	3.67 2.05	-	3.61 1.92	-	-	-	3.68 2.09
Methyl Iodide	s	2.16	-	2.21	-	-	2.15	insol
Morpholine	m m	3.69 2.85	-	3.52 2.68	-	3.64 2.79	3.70 2.79
nitromethane	s	4.33	4.43	4.42	2.94	4.31	4.34	4.40
n-pentane	t, 7 m	0.88 1.27	0.88 1.27	0.86 1.27	0.87 1.23	0.89 1.29	0.90 1.29	-
Propane-1,2-diol	d, 6	1.17	-	1.04	-	-	-	1.13
Propionoic Acid	q, 7 t, 7	2.42 1.18	-	2.26 1.03	-	-	-	2.47 1.10
2-propanol	d, 6 sep, 6	1.22 4.04	1.10 3.90	1.04 3.78	0.95 3.67	1.09 3.87	1.50 3.92	1.17 4.02
pyridine	m m m	8.62 7.29 7.68	8.58 7.35 7.76	8.58 7.39 7.79	8.53 6.66 6.98	8.57 7.33 7.73	8.53 7.44 7.85	8.52 7.45 7.87
Pyridine.HCl	m m m	-	-	-	-	-	8.92 8.19 8.69	-
silicone grease	s	0.07	0.13	-	0.29	0.08	0.10	-
Succinimide	s	2.75	-	2.63	-	-	-	2.78
1,1,2,2-Tetrachloroethane	s	5.96	-	6.92	-	-	-	insol
tetrahydrofuran	m m	1.85 3.76	1.79 3.63	1.76 3.60	1.40 3.57	1.80 3.64	1.87 3.71	1.88 3.74
toluene	s m m	2.36 7.17 7.25	2.32 7.1-7.2 7.1-7.2	2.30 7.18 7.25	2.11 7.02 7.13	2.33 7.1-7.3 7.1-7.3	2.32 7.16 7.16	-
1,1,1-Trichloroethane	s	2.72	-	2.80	-	-	-	insol
triethylamine	t, 7 q, 7	1.03 2.53	0.96 2.45	0.93 2.43	0.96 2.40	0.96 2.45	1.05 2.58	0.99 2.57
Water	s	1.60	-	3.40	-	-	-	4.60
Solvent	Multiplicity	CDCl₃	(CD₃)₂CO	(CD₃)₂SO	C₆D₆	CD₃CN	CD₃OD	D₂O